Beamline 5-ID-B,C,D: Sector 5 - Insertion Device
DND-CAT
Materials Science, Polymer Science, Chemistry, Life Sciences
Description
The 5-ID beamline contains three end stations for use by general users.
The 5-ID-B station contains a custom 11-detector powder camera. This system has 11 Si(111) analyzer crystals and operates at an energy of ~ 17.5 keV for high-resolution powder diffraction measurements. The system has a six-position sample changer for capillaries. WAXS measurements with a MAR165 detector can also be performed.
The 5-ID-C station has two instruments, a kappa diffractometer for in-air or small sample environment cells, and a UHV chamber with MBE, photoelectron detection up to 10000 eV, and other capabilities. This station has post-monochromator optics for beam conditioning primarily for x-ray standing wave measurements. The UHV system and the post-monochromator optics are only available to general users in a collaborative mode.
The 5-ID-D station contains a pinhole small-angle x-ray scattering (SAXS) camera with a maximum sample-to-detector distance of approximately 7.5 m. Simultaneous small-, medium- and wide-angle diffraction (SAXS/MAXS/WAXS) with custom Rayonix fast frame-transfer CCD detectors is available on 5-ID-D, including an optional in-vacuum flow cell for solution SAXS/MAXS/WAXS.
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Supported Techniques
- Powder diffraction
- X-ray standing waves
- X-ray optics development/techniques
- Small-angle x-ray scattering
- Surface diffraction
- X-ray reflectivity
- Wide-angle x-ray scattering
Beamline Controls and Data Acquisition
EPICS for motors and actuators on all systems. SPEC used to control diffractometers. Vendor-supplied software used to control CCD detectors. Real-time data reduction for SAXS/MAXS/WAXS system.
Detectors
- Scintillation detectors
- Mar 165 mm CCD detector
- Microphotonics GEMSTAR 2-D detector
- Rayonix SAXS/MAXS/WAXS system
- 11-detector powder camera
- Vortex Silicon Drift Detector
Additional Equipment
- Small kappa 5-circle diffractometer
- Capillary lens
- In-vacuum SAXS/MAXS/WAXS setup
- Simultaneous SAXS/MAXS/WAXS
- Instron servo-hydraulic tensile stage (collaboration only)
- Solution SAXS in-vacuum flow cell
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Local Contacts
Beamline Specs
Source |
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Monochromator Type |
Si(111) |
Energy Range |
6-35 keV |
Resolution (ΔE/E) |
1 x 10 -4 |
Flux (photons/sec) |
1 x 10 13 @12 keV |
Beam Size (HxV) |
Focused |
50µm x 1000µm
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Unfocused |
1mm x 1mm
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For additional information see:
https://www.dnd.aps.anl.gov/
Current Status:
Operational/Accepting General Users
Access Mode:
On-site
Mail-in
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