Beamline 11-ID-D: High-energy X-ray Diffraction & Small Angle Scattering
X-ray Science Division, APS
Materials Science, Environmental Science, Physics
Description
11-ID-D will offer a wide range of experimental approaches with the highest available flux. Two dimensional focusing will be available with adaptable energy resolution. A q-range from 0.01A-1 to 40A-1 will be covered. The photon energy will cover the entire range from 26 to 130 keV. A secondary detector for spectroscopic/ Compton imaging will expand the multimodal approaches.
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Supported Techniques
- High-energy x-ray diffraction
- X-ray total scattering, pair distribution function (PDF)
- Grazing incidence diffraction
Beamline Controls and Data Acquisition
Linux workstation running SPEC; EPICS;
QXRD for data acquisition
GSAS-II and xPDFsuite for data processing
Fit2D, pdfgetx2, and pdfgetx3
Detectors
- Pilatus 2M
- Perkin Elmer XRD 1621 amorphous silicon detector
- Varex 4343CT (150 micron pixel size)
Additional Equipment
- 2D focusing (>0.5 um x 0.5 um)
- Flowcell/Controlled Atmosphere (RT to 1000C)
- Multiple-sample furnace (RT to 400C)
- Vertical furnace for melts (RT to 1000C)
- Oxford Cryostream 800+ (80K-500K operations)
- Electrochemistry cells thru APS E-Chem Lab
- Programmable Mass Flow Controllers
- Residual Gas Analyzer (with advanced notice)
- PI Hexapod
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Local Contacts
Beamline Specs
Source |
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Monochromator Type |
Multilayer + secondary mono |
Energy Range |
26-120 keV |
Resolution (ΔE/E) |
2 x 10 -4 |
Flux (photons/sec) |
1 x 10 13 @65 keV |
Beam Size (HxV) |
Focused |
.5µm x .5µm
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Unfocused |
.5mm x .5mm
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For additional information see:
https://www.aps.anl.gov/Structural-Science
Current Status:
Construction
Access Mode:
On-site
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